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Research Article
Yao Liu
Pingxiang University
Corresponding Author
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This work is licensed under a CC BY 4.0 License. Read Full License
The densification mechanism of doped CeO with Si3N4 powder during Spark Plasma Sintering (SPS) was investigated under temperatures ranging from 1500 to 1750 °C at soaking pressures of 30, 40, 50 MPa. Results showed that the relative density of Si3N4 ceramics sintered at 1650 °C and 30 MPa was 97.9%. A creep model was employed to determine the mechanism, which can be interpreted on the basis of the stress exponent (n). The results showed that the mechanism was controlled by liquid phase sintering at low effective stress regime (n=1).
Keywords
SPS, Si3N4 ceramics, Doped, Liquid phase sintering
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This is a preprint, a preliminary version of a manuscript that has not completed peer review at a journal. Research Square does not conduct peer review prior to posting preprints. The posting of a preprint on this server should not be interpreted as an endorsement of its validity or suitability for dissemination as established information or for guiding clinical practice.
Research Article
Yao Liu
Pingxiang University
Corresponding Author
Badges
Prescreen
This manuscript passed our Prescreen assessment
Complete author information
Appropriate declaration statements
Potential risks to human health
Prescreen
History
CURRENT STATUS: Posted
Version 1
Posted 04 Jan, 2021
No community comments so far
Metrics
Comments: 0
PDF Downloads: ...
HTML Views: ...
Subject Areas
Mechanical Engineering
License:
This work is licensed under a CC BY 4.0 License. Read Full License
The densification mechanism of doped CeO with Si3N4 powder during Spark Plasma Sintering (SPS) was investigated under temperatures ranging from 1500 to 1750 °C at soaking pressures of 30, 40, 50 MPa. Results showed that the relative density of Si3N4 ceramics sintered at 1650 °C and 30 MPa was 97.9%. A creep model was employed to determine the mechanism, which can be interpreted on the basis of the stress exponent (n). The results showed that the mechanism was controlled by liquid phase sintering at low effective stress regime (n=1).
Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
This preprint is available for download as a PDF.
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