Effect of cryogenic and electrolytic passivation treatment on wear resistance of M2 high-speed steel

Through cryogenic treatment and electrolytic passivation treatment of M2 high-speed steel (HSS), the effect of electrolytic passivation process parameters on the life of M2 HSS taps and the combined effect of cryogenic treatment and electrolytic passivation treatment on the wear resistance of the M2 HSS were investigated by using a scanning electron microscope (SEM) and energy-dispersive spectrometer (EDS). The results show that the life of M2 HSS tap after electrolytic passivation treatment increases most significantly under the theoretical edge radius; the functional relationship between the charge consumption (y) and the tap edge radius (x) is as follows: y = 8.135x − 48.842. The wear resistance of the sample after cryogenic and electrolytic passivation treatment is the highest, which is 1.52 times higher than those of the traditional heat treatment sample. This is due to the increase of the number of carbides on the surface of the specimens after cryogenic treatment; the distribution and size of carbides are relatively uniform; the average size of carbides is reduced by 60.4%. There is a carbon layer on the surface of the sample after passivation, which can effectively improve the wear condition. The size and number of carbides in the surface layer of the sample remain unchanged after passivation treatment, indicating that cryogenic treatment plays a key role in the performance of the material.


Introduction
As a high alloy tool with high hardness, HSS is widely used in various sophisticated tools such as taps, drill bits, and broach cutters [1].
Cryogenic treatment is an extension of the heat treatment process, which has also been shown to significantly improve the material properties of HSS cutting tools [2]. After cryogenic treatment, HSS tools exhibit superior wear resistance and dimensional stability [5]. The increase of cryogenic technology in the industrial field has greatly extended the HSS service life [8]. The cryogenic treatment is an effective method to improve the wear resistance of M2 steel, and studies show that 77 K cryogenic temperature and extension of cold holding time to 24 h can significantly increase its wear resistance [9]. The service life of the M2 HSS drill is increased by 126% after being immersed in liquid nitrogen for 24 h and then tempered at 473 K. The cryogenic treatment not only promotes the transformation of retained austenite to martensite but also uniformly precipitates elliptical carbide particles, which enhances the service life of highspeed steel tools [10].
Since micro-defects such as burrs and openings often exist in HHS tools such as taps after sharpening, electrolytic passivation is a common solution to a series of problems such as micro-cracks, uneven surface, and unstable. cutting performance caused by sharp edges. The edge of the tap is smoother after electrolytic passivation, and the roughness of the rake face of the cutting tool is significantly reduced, which can improve the service life of HSS taps [11]. The feasibility of the electrolytic passivation treatment carried out the electrolytic passivation treatment for cemented carbide cutting tools to eliminate the micro-defects of the cutting tools and improve the surface quality of the workpiece [12]. The changes of tangential force, radial force, and friction force in cutting titanium alloy at different cutting edge radius and cutting speeds found that the friction force when cutting titanium alloy is not only affected by the cutting speed but also related to the value of cutting edge radius of the tool [13]. However, the relationship between electrolytic passivation process parameters and the service life of HSS taps and the mechanism of the combined effect of electrolytic passivation and cryogenic treatment on the wear resistance of HSS has not been studied in depth. Therefore, the electrolytic passivation treatment of M2 HSS taps is used to establish the relationship between the electrolytic passivation process parameters and tap life, optimize the electrolytic passivation process parameters, and perform electrolytic passivation and cryogenic treatment on M2 HSS to reveal the evolution mechanism and organization of the wear resistance of HSS by electrolytic passivation and cryogenic treatment, and to provide guidance for industrial applications. A TYESM-15 electrolysis equipment independently developed by the laboratory with a 500-mm cell capacity was used for passivation with the voltage and current ratings of 220 V and 0-10 A, respectively; cutting tool diameters of 3-12 mm; and spindle speeds of 0-120 r/min. The sample is clamped in the electrolytic anode, and phosphoric acid solution is used as an electrolyte. During electrolytic passivation, the whole process is automatically controlled by the program. After the electrolysis passivation test, the sample was neutralized in 5% Na 2 CO 3 solution, and then cleaned in water.

Theoretical dimensions of tool edge radius
Electrolytic passivation treatment can eliminate the unevenness of the tap edge and improve the tap edge radius to increase the life of the tap. The relationship between the theoretical edge radius size of the tap and the tool angle is shown in Fig. 1 [14].where r is the edge radius, 0 is the front angle, and 0 is the back angle. The unevenness of the cutting edge applicable to most cutting tools ranges from 0.01 to 0.05 mm; the edge unevenness takes the minimum value of 0.01 and the maximum value of 0.05 accordingly, so the range of edge radius is 0.016-0.060 mm. Given that the tap is a small precision tool with multiple cutting edges, the cutting part of the cutting edge is short, the radius of the cutting edge will be blunted if the reference is based on the standard of other tools, the value of the edge radius of the tap should be smaller, and the value of the blunt radius is 0.016 mm.

Relationship between electrolytic passivation process parameters and tap edge radius
The main adjustable. electrolytic parameters of the electrolytic passivation equipment used in this experiment are electrolytic power consumption, in Coulomb (C). The relationship between Coulomb C and the tap edge radius is established. The basic test environment is as follows: the electrolytic power supply is 12 V DC high-frequency pulse power supply, the spindle speed is 120 rpm, the electrolyte is the phosphoric acid solution, and the electrolyte temperature is 25 ℃. Six groups of taps with an electrolytic power consumption of 100 C, 200 C, 300 C, 400 C, 500 C, and 600 C were tested for passivation, with three taps in each group.  Table 1; the passivation effect of different electrolytic power consumption on the tap edge is shown in Fig. 2. As can be seen from Fig. 2, after electrolytic passivation, the tap presents different degrees of blunt and the edges become round. At the same time, due to the fast discharge rare of the tip of the tap, the dissolution speed is also fast, making the surface flat. When the energized charge is high, the surface will be dissolved to produce very many small pits, which is very beneficial for the storage of cutting fluid.
A scatter plot of electrolytic passivation power consumption versus tap edge radius was plotted and fitted as a function by the MATLAB software, as shown in Fig. 3. The function between the charge quantity (y) and the tap edge radius (x) is y = 8.135x − 48.842.

Effect of edge passivation on life of M2 HSS tap
According to the function, it can be seen that the theoretical edge radius of this type of tap is 16 μm, and the corresponding electrolysis parameters are near 75 C. Therefore, the electrolysis parameters for this test are 0 C, 50 C, 75 C, 100 C, 150 C, and 200 C, of which 0 C is the comparison group without passivation.
The six groups of taps were tapped after the above electrolytic passivation treatment to study the relationship between the electrolytic passivation process parameters and the life of HSS taps. WMD0912 Wanmuchun brand tapping machine was used in this experiment. The tapping cutting speed was 10.807 m/min (spindle speed 430 r/min). The processed material was H13 steel, processing method selected through-hole processing, bottom hole diameter of 6.8 mm, and tap failure criteria by measuring maximum  [15]. As shown in Fig. 4, the maximum wear values of the taps' flank face were recorded for six groups of taps when machining 10, 20, 40, and 60 holes, respectively. From this diagram, it can be seen that the overall wear trend of the six groups of taps is roughly in line with the typical three stages of flank face wear: initial wear stage, normal wear stage, and rapid wear stage.
In the initial wear stage, the wear rate of the unpassivated tap is the fastest, and the back tool surface presents the form of groove wear. After machining 10 holes, the wear has reached the maximum among the 6 groups of taps, while the other groups of passivated taps all wear slower than the unpassivated taps. The reason for the faster wear rate of the 200-C passivation taps is due to the instability of the cutting process and the vibration of the spindle caused by a large amount of passivation and the blunt edge, which aggravates the wear of the tap.
In the normal wear stage, due to the defects of the unpassivated taps themselves, the whole life cycle is short and the wear rate is very fast. The normal wear phase is not obvious, and the effective time of work is very short, and it also indicates that the quality of the unpassivated taps for machining holes is not stable. The 150-C passivated tap has reached the wear standard before 40 holes due to the cutting heat and poor chip removal during continuous machining.
The rapid wear stage should be avoided as much as possible. The unpassivated tap has already reached the rapid wear stage, and there are abnormal failure forms such as large-scale chipping. Due to the extension of the normal wear stage of the 50 C, 75 C, and 100 C passive taps, the rapid wear stage is not obvious during the effective working period, which largely avoids the abnormal failure mode. The wear rate of the passivated taps at this phase is also significantly lower than that of the non-passivated taps.
Based on the above experimental results and analysis, when the electrolytic passivation charge is 75 C, that is, the tap edge radius is about 17 μm, the life of the tap has the highest improvement. The wear resistance is better at the initial stage of wear, the normal wear stage is prolonged, the effective working time is increased, and the working efficiency is improved. To a certain extent, the rapid wear stage is avoided, and the abnormal wear form is greatly alleviated. The processing is stable and reliable, and the passivation effect is the best.

Sample materials and preparation
In order to study the effect of cryogenic treatment and electrolytic passivation on the wear resistance of M2 HSS, two types of samples were selected. The first type dimension was φ40 × 10 mm. The size of the second type was 5 × 5 × 10 mm 3 , cut from the first type after the experiment.

Heat treatment and cryogenic treatment process
According to the summary of the cryogenic test at the early stage, it is considered that the toughness and wears resistance can be well balanced by the cryogenic treatment before tempering, which aims to improve the service life and cutting performance of HSS taps [7]. In this experiment, the quenching and tempering treatments were conducted in a vacuum furnace (VHQ-122 l-06, Shenyang Jayu vacuum technology Co. Ltd, Shenyang, China). To balance the macro-properties, the quenching temperature is set at 1483 K. Cryogenic treatment was conducted by our homemade cryogenic equipment (TYKD-1, Taiyuan University of Technology and Science, Taiyuan, China). The cryogenic temperature was set at 118 K for 360 min, which cooling rate is 1 K/min. Tempering temperature is selected as 833 K. According to the traditional heat treatment process of HSS, there were three times conventional tempering treatments, which the heat preservation was carried out for 60 min. All details were shown in Fig. 5.

Electrolytic passivation treatment process
The electrolytic passivation treatment was performed in an electrolytic passivation apparatus (TYESM-15). The sample under test was clamped in the electrolytic anode, and the power consumption, current, and voltage were set to 1000 C, 10 A, and 10 V, respectively.

The experimental scheme of M2 HSS material
The experimental program includes traditional heat treatment group (QT), traditional heat treatment + deep cooling treatment group (QCT), traditional heat treatment group + electrolytic passivation group (QTP), and traditional heat treatment + deep cooling treatment + electrolytic passivation group (QCTP). Based on the experimental results previously published by the research group, the experimental schemes include the QT group, the QTP group, the QCT group, and the QCTP group [17]. The experimental scheme is shown in Table 2, and there are 3 samples in each group. The schematic diagram of cryogenic treatment and electrolytic passivation is shown in Fig. 6.

Wear test
According to the experimental scheme, the grinding process was finished on the "M7130" surface grinding machine (M7130, Beijing North First machine tool Co. Ltd, Beijing, China) after the tempering process; the surface roughness was under 0.8 μm. Samples were finished on the polishing machine (PG-1, Chinese Nanjing Lianchuang Analytic Instrument Co. Ltd, Nanjing, China) after grinding process. The samples were put into an ultrasonic cleaning machine to clean with acetone solution before the wear test. Then, there were three samples in each group, which need to be strengthened by electrolytic strengthening treatments. Tapping can be simply regarded as the friction pair formed by tap and workpieces. The purpose of the wear test is to simulate the wear condition and explain the impact of wear conditions on the material properties, which is to select the optimal process and process parameters [19]. According to tapping process simulation by a research group in an earlier stage, the tapping highest temperatures could be 773 K. The test parameters are selected according to the working conditions of high-speed steel tap tapping [22]. A ball-ondisc high-temperature (

Microscopic analysis
After the macro-properties test, the samples were cut into the second type. The second type has two types of samples, which were samples including wear scars (WS) and samples without wear scars (WWS).
The observation surface of WWS samples was polished with abrasive paper to make the surface free from scratches. Then, the PG-1 metallographic polishing machine was used for polishing. Chromium trioxide was used as the polishing powder, which was polished to the bright surface. The metallographic corrosion was carried out on the observation surface with an 8% nitric acid alcohol solution. Finally, a scanning electron microscope (SEM) and an energy dispersive spectrometer (EDS) were used to observe the carbides precipitation status of samples.
The WS samples were cleaned in acetone solution at room temperature for 30 min. The surface morphology of wear scars was observed with an optical microscope to ensure that they were clean. The wear scars were observed by SEM, and the wear mechanism was speculated by EDS.  QT  1483  293  0  833  N  QTP  1483  293  0  833  Y  QCT  1483  118  3  833  N  QCTP  1483  118  3 833 Y Fig. 6 The schematic diagram of cryogenic treatment and electrolytic passivation 4 Results and discussion

The influence in different processes on friction coefficient
To make the test results more impartial, there are three samples in each group and the final friction coefficient consists of the average of the three friction coefficients at each collection time point. Figure 7 shows the variation of the friction coefficient for four groups of specimens with a wear time of 60 min. It can be seen from the Fig. 7 that: (1) The friction coefficient before and after cryogenic was compared. Comparing the friction coefficient curves of the QT group and QCT group, the friction coefficient of QCT group specimens after deep cooling treatment is lower than that of QT group specimens without deep cooling treatment. The friction coefficient of the QT group had a periodic trend of repeated cycle rise and sudden drop, fluctuating between 0.65 and 0.71. There was no significant difference in the time required for the two groups of samples in the pre-grinding stage, which was about 3~4 min. After entering the normal wear stage, the friction coefficient of the QCT group after cryogenic treatment fluctuated slightly, and the final friction coefficient decreased to about 0.55. (2) Comparison of friction coefficients before and after electrification. Comparing the friction coefficient curves of the QT group and QTP group, the friction coefficient of specimens in the QTP group after electrolytic passivation is lower than that of specimens in the QT group without electrolytic passivation. In the early stage of friction, the friction coefficient of the QTP group after electrolytic passivation was larger than that of the QCT group after cryogenic treatment. However, after 30 min, the friction coefficient of the QTP group fluctuated up and down in the friction coefficient curve of the QCT group, and the average friction coefficient of the QTP group was 0.124 lower than that of the QT group. (3) For the friction coefficient curve of the QCTP group, it was slightly higher than that of the QTP group and the QCT group at the first 30 min, but after a small range of shock for 20 min, it was stabilized near 0.5 at the late stage of wear, and the average friction coefficient of QCTP group was reduced by 0.151 compared with that of QT group. (4) By comparing the friction coefficient curves of the four groups, it can be seen that both cryogenic treatment and electrolytic passivation can effectively reduce the friction coefficient value during high-temperature wear. The friction coefficient value of the specimen after cryogenic treatment has a significant tendency to decrease, and the specimen will have a black carbon layer on the surface of the specimen after electrolytic passivation treatment, as shown in Fig. 8. It is preliminarily judged that the reason for the appearance of the carbon layer is that during the electrolytic passivation process, the sample was used as an anode. After the metal atoms on the surface of the sample lost electrons and became metal cations into the solution, the residual carbon atoms on the surface of the sample had a certain lubrication effect, so the friction coefficient of the sample after electrolytic passivation treatment could be effectively reduced. Cryogenic treatment and electrolytic passivation treatment are superimposed for better wear resistance, but the decisive role is played by the cryogenic treatment, and electrolytic passivation cannot significantly expand this advantage.

The influence in different processes on relative wear resistance
Relative wear resistance E = W A /W B refers to the ratio of wear amount of two different materials under the same wear condition. The wear amount of one material sample is taken as the standard. W A is the volume loss of standard samples; W B is the volume loss of the target samples [23]. Each group's wear volumes were measured in CFT-I material surface performance comprehensive test instrument. Table 3 shows the changes of relative wear resistance of different processes. It can be seen from Table 3 that the relative wear resistance of the QTP group, the QCT group, the QCTP group, and the QT group was 1.09, 1.34, and 1.52 times higher than that of the QT group, respectively. It was further verified that both electrolytic passivation and cryogenic treatment can improve the wear resistance of M2 HSS, but the decisive role is played by the cryogenic treatment.

Wear scar analysis
To illustrate that cryogenic treatment and electrolytic passivation treatments can effectively improve the wear resistance of M2 HSS, wear scars were observed under an optical microscope.
The ImageJ software was used for image processing of the wear scars. Table 4 shows the area of wear scars (AWS), the average size of wear scars (ASWS), and the percentage of wear scars sizes (PWSS). Figure 9 shows the SEM images of the wear scars of the four groups of samples after hightemperature wear and the corresponding element contents measured by EDS.
It can be seen from Table 4 that the surface wear of the QT group sample is serious, with the largest ASWS, and the PWSS is 61.2%. After cryogenic treatment, the wear scar of the QCT group is significantly reduced, and the ASWS is relatively small, with the PWSS of 30%. After electrolytic passivation treatment, the ASWS of the QCP group can also be reduced by nearly 48%. It shows that cryogenic treatment and electrolytic passivation treatment can effectively alleviate the wear, and the QCTP group after cryogenic treatment and electrolytic passivation treatment has the best effect.
From Fig. 9, it can be seen that: Figure 9a, b show the SEM and the EDS diagrams of the wear scars of the QT group samples. It can be seen from Fig. 9a that this group of samples is the most seriously worn one of the four groups of samples, which is reflected in the large area of dark black plow mark trauma morphology. The dark black oxidation marks are continuous and large area, and many spherical particle debris are attached to the wear surface, and the plowing material is stacked on both sides of the groove in a large amount and accompanied by the traces of material flaking off in a whole piece. From Fig. 9b, it can be seen that the surface layer of the specimen contains a high content of oxygen and tungsten elements, indicating the presence of oxidative wear on the surface layer as well as the exposure of the inner matrix after the damage by adhesive wear. Therefore, the wear mechanism of this group is mainly abrasive wear and adhesive wear, and the degree of oxidation wear is generally serious at 773 K. In comparison, the most typical wear forms in this group are still abrasive wear and adhesive wear. Figure 9 c, d show the SEM and the EDS diagrams of the wear scars of the QCT group samples. It can be seen from Fig. 9c that after cryogenic treatment, the surface wear morphology of the sample was improved compared with that of the QT group. The main manifestations were that the groove wear traces were less and deeper, the furrow area was small and incoherent, and a small amount of soft material had obvious traces of tearing down the whole oxide layer. As can be seen from Fig. 9d, the higher content of carbon elements in this group of specimens indicates that more carbide precipitates in the surface layer after cryogenic treatment, Fig. 8 Morphology of the samples before and after passivation treatment  which helps to reduce the degree of wear damage. The main wear mechanisms are oxidation wear and adhesive wear, as well as lighter abrasive wear. Figure 9e, f are the SEM and EDS images of the wear scars of the QTP group. Fig. 9e, f are the SEM and EDS images of the wear scars of the QTP group. The results show that after electrolytic passivation, the furrows on the surface of the sample are lighter, and there are a small amount of traces of the oxide layer peeling off on the surface, and the content of the C element in the surface is 3 times that of the unpassivated sample. It shows that after electrolytic passivation, the surface metal atoms become free metal ions under the action of electrolyte, and the remaining C atoms in the surface increase the lubrication effect of friction. The main wear mechanisms are oxidation wear and slight abrasive wear and adhesive wear. Figure 9 g, h are the SEM and EDS diagrams of the wear scars of the QCTP group samples, from which it can be seen that the group specimens have more traces of oxide layer peeling off after deep cooling and electrolytic passivation treatment, and the content of oxygen and iron elements are higher, indicating that after the oxide peels off from the surface layer through fatigue wear, the presence of abrasive chips between the two wear surfaces plays a weak role in reducing wear and effectively relieves wear. Therefore, it can effectively reduce the friction coefficient in the late stage of frictional wear. At the same time, the content of the C element increased from 8.7% of the QT group to 18.9%, which Fig. 9 SEM photos of the wear scar of four groups of different processed samples. a, b worn surface morphology and its corresponding EDS spectrum of the QT group samples. c, d worn surface morphology and its corresponding EDS spectrum of the QCT group samples. e, f worn surface morphology and its corresponding EDS spectrum of the QTP group samples. g, h worn surface morphology and its corresponding EDS spectrum of the QCTP group samples also played a role in lubricating the friction surface. The main wear mechanism is oxidation wear.

Microstructure
In the past, the researches of HSS wear performance mainly focused on the different heat-treatment processes. Now, cryogenic treatment is generally recognized by the heat treatment field, which especially generates the greatest effect in the carbides precipitation of HSS [24]. The cryogenic treatment provides the driving force for transformation from residual austenite to martensites, which increases the number of fine martensite and reduces the rate of lattice distortion. The smaller the size of carbides is the better strengthening effect it generates. The carbides are divided into primary carbides (FC: size 5 > μm) and secondary carbides (SC: size ≤ 5 μm). The size of the carbide is 1 ~ 5 μm, which is seen as the large secondary carbides (LSC). The size is 0.1 ~ 1 μm, which is seen as the small secondary carbides (SSC) [3]. The more secondary carbides there are, the better material properties will be. Figure 10 is the four group's carbide images taken by scanning electron microscopy (SEM) at 3000 times. The white matters in the pictures are carbides. We can count the number and size of carbide particles by the ImageJ software, and the specific data were shown in Page 16, Table 5; the mean carbide value of the QCTP group was reduced by about 60.4% compared to the mean value of the QT group. Figure 10 intuitively shows the distribution of carbide particles. Many primary carbides are precipitated from liquid steel during the process of condensation, which is eutectic and hypereutectic carbides. Secondary carbides are precipitated from the solid matrix during heat treatment or other treatment processes. Therefore, it can be seen that the fine carbide is precipitated at the grain boundary and distributed on the matrix.
According to Fig. 10 and Table 5, we should pay attention to the proportion that the number of different type's carbides accounts for the total number. It can see clearly that the total number of the first group is much lower than the other three groups. Carbide distribution is very sparse. There are some segregation phenomenons of carbide, and many matrices do not exist carbide. The proportion of primary carbides was 5.7%, large secondary carbides were 44.3%, and small secondary carbides were only 50%, which is far lower than the other three groups. The stacking of carbides will lead to the stress concentration of materials. Many primary carbides could not improve the performance of steel, which will waste  alloy elements and reduce the utilization rate of alloy. The average size of carbide was as high as 1.342, which is much higher than other groups. As for the principle of cryogenic treatment leading to the precipitation of small secondary carbides, the mainstream believes that the transformation of carbides is activated by the cryogenic treatment in this field. The generation of tempered martensite is also accompanied by the precipitation of small carbides, and the release of energy improves the nucleation rate of carbides. The small secondary carbides present a spherical shape after cryogenic treatment. The total numbers of the second group carbide are 244. The carbide distribution and size are relatively uniform, which the primary carbide accounts for 0.8% of the total number, large secondary carbides account for 5.3%, and small secondary carbides account for 93.8%. The average size of the carbide is about 0.473, so wear resistance is relatively good than the fourth group. Small particles of dispersion carbide are distributed in the matrix and grain boundaries, and the dispersion is more uniform than the other three groups, which effectively improves the wear resistance of M2 HSS.
It can be seen from Fig. 10c and d that the size and number of carbides remain unchanged before and after passivation treatment, which indicates that the internal structure of the material will not change after electrolytic passivation treatment. Cryogenic treatment plays a key role in material performance.

Conclusions
The effect of electrolytic passivation process parameters on the life of M2 HSS taps and the combined effect of cryogenic treatment and electrolytic passivation treatment on the wear resistance of M2 HSS was investigated. The results obtained in the present investigation assist to infer the following major conclusions: (1) Through the electrolytic passivation treatment and tapping experiment of M2 HSS tap, it is concluded that the life of M2 high-speed steel tap after electrolytic passivation treatment is the most obvious under the theoretical tap edge radius; the function between the charge quantity (y) and the tap edge radius (x) is y = 8.135x − 48.842. It can be used to guide industrial mass production and improve production efficiency and service life of tap tools. (2) The surface of samples with electrolytic passivated appears a layer of graphite. Based on the property of lubrication of graphite, the wear resistance of samples with electrolytic strengthening was improved. The normal wear stage of the flank is effectively prolonged.
(3) The high-temperature wear forms of the traditional heat specimens are mainly abrasive wear and adhesive wear, while the high-temperature wear forms of the specimens after cryogenic treatment and electrolytic passivation treatment are mainly oxidation wear and slight adhesive wear. (4) The wear resistance of cryogenically treated samples is better than that of non-cryogenic treated samples, which is due to the increase of secondary carbide content. Electrolytic passivation treatment can also improve the wear resistance of the sample, but after electrolytic passivation treatment, the internal structure of the material does not change, and cryogenic treatment plays a key role in material performance.
Author contribution All authors contributed to the study conception and design. Material preparation and data collection were performed by Xianguo Yan, Jiale Li, and Fan Li. The data analysis was performed by Zhi Chen and Yangwei Zhang. The first draft of the manuscript was written by Zhi Chen, and all authors commented on previous versions of the manuscript. All authors read and approved the final manuscript.
Funding The authors received financial support from the Natural Science Foundation of China (NSFC) (No. 51275333).
Data availability Not applicable.
Code availability Not applicable.

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Competing interests
The authors declare no competing interests.