An extensive multi-year experimental study was conducted to investigate the potential production of deuterium from titanium hydride (TiHx) powders subjected to specific thermal cycles. The results reveal an anomaly in the deuterium-to-hydrogen ratios. Mass spectrometry analyses show an increase in deuterium abundance, with three independent methods confirming the excess deuterium. This study was motivated by theoretical predictions suggesting the generation of slow neutrons within metal hydrides when exposed to coherent excitations. Our findings align with direct measurements of neutron emission by TiHx powders under cavitation in liquid water, as recently published by Fomitchev-Zamilov.