This is a preprint, a preliminary version of a manuscript that has not completed peer review at a journal. Research Square does not conduct peer review prior to posting preprints. The posting of a preprint on this server should not be interpreted as an endorsement of its validity or suitability for dissemination as established information or for guiding clinical practice.
A new preprint design is coming!
We have improved readability, clarity, accessibility, and opportunities for engagement.
Research Article
Dilek Çanakçı
Adıyaman University
Corresponding Author
License:
This work is licensed under a CC BY 4.0 License. Read Full License
In this study, hydroxyapatites reinforced with Boron, Copper and Zinc at different rates were produced using the sol-gel method. Different amounts of metal during the production of hydroxyapatite were used to observe the amount of crystallization and morphological differences in their structures. The characterization of the metal-doped HAp was carried out by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDX). The data indicated that the Ca/P stoichiometric ratios of the samples varied between 1.71 and 2, so their morphologies were different from each other. The absorption behavior of novel metal-doped HAp samples was evaluated at room temperature by UV-vis spectroscopy. In the absorption spectra of the samples, absorption bands formed in similar regions. In addition, the thermal behavior of HAp samples was investigated using TG/DTA techniques. The results of the analysis showed that heat resistance of the new synthesized samples was quite high.
Keywords
hydroxyapatites, Boron, Copper, Fourier transform infrared (FTIR)
Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11
Figure 12
Figure 13
Figure 14
Figure 15
Figure 16
Figure 17
Figure 18
Figure 19
Loading...
Badges
Prescreen
This manuscript passed our Prescreen assessment
Complete author information
Appropriate declaration statements
Potential risks to human health
Prescreen
History
CURRENT STATUS: Posted
Version 1
Posted 14 Jan, 2021
No community comments so far
Metrics
Comments: 0
PDF Downloads: ...
HTML Views: ...
Subject Areas
Physical Chemistry
Learn more about our company.
A new preprint design is coming!
We have improved readability, clarity, accessibility, and opportunities for engagement.
This is a preprint, a preliminary version of a manuscript that has not completed peer review at a journal. Research Square does not conduct peer review prior to posting preprints. The posting of a preprint on this server should not be interpreted as an endorsement of its validity or suitability for dissemination as established information or for guiding clinical practice.
Research Article
Dilek Çanakçı
Adıyaman University
Corresponding Author
Badges
Prescreen
This manuscript passed our Prescreen assessment
Complete author information
Appropriate declaration statements
Potential risks to human health
Prescreen
History
CURRENT STATUS: Posted
Version 1
Posted 14 Jan, 2021
No community comments so far
Metrics
Comments: 0
PDF Downloads: ...
HTML Views: ...
Subject Areas
Physical Chemistry
License:
This work is licensed under a CC BY 4.0 License. Read Full License
In this study, hydroxyapatites reinforced with Boron, Copper and Zinc at different rates were produced using the sol-gel method. Different amounts of metal during the production of hydroxyapatite were used to observe the amount of crystallization and morphological differences in their structures. The characterization of the metal-doped HAp was carried out by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDX). The data indicated that the Ca/P stoichiometric ratios of the samples varied between 1.71 and 2, so their morphologies were different from each other. The absorption behavior of novel metal-doped HAp samples was evaluated at room temperature by UV-vis spectroscopy. In the absorption spectra of the samples, absorption bands formed in similar regions. In addition, the thermal behavior of HAp samples was investigated using TG/DTA techniques. The results of the analysis showed that heat resistance of the new synthesized samples was quite high.
Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11
Figure 12
Figure 13
Figure 14
Figure 15
Figure 16
Figure 17
Figure 18
Figure 19
Loading...